MANUFACTURE OF LSD Materials: 1. Ergotamine tartrate 2. Hydrazine hydrate 3. Hydrazide 4. Hydrochloric Acid 5. Sodium Nitrite 6. Sodium Bicarbonate 7. Diethylamine 8. Ether 9. Flasks 10. Filter paper 11. Heating mantle 12. 2 liter three-necked round bottom flask Time: Approximately 36 hours. Process: STEP 1: In a 2 liter three-necked round bottom flask add to 2 grams of ergotamine tartrate about 1/2 gram of hydrazine hydrate. Exercise caution when adding the hydrazine hydrate because it is very poisonous, particularly to the eyes. STEP 2: Place a condensing column on one neck of the flask. Place a stirring device in the center neck and place a separatory funnel in the thick neck. (Note: hydrazide hydrate may be added through a separatory funnel although it is not necessary.) STEP 3: Place the flask on a heating mantle and simmer the solution for 2-3 hours while stirring occasionally. STEP 4: Remove condensing column from flask and continue to cook for 10-15 minutes or until the original solution is reduced by half. STEP 5: After solution has cooled, pour the solution through filter paper and collect the crystals that formed. Wash the crystals in a small amount of absolute alcohol. STEP 6: Dissolve the crystals in about 30cc of diluted hydrochloric acid. (Note: diluted hydrochloric acid is mixed at a rate of 1 part acid to 10 or 15 parts water.) STEP 7: To the hydrochloric acid solution add about 15cc of a solution of sodium nitrite diluted in water. (Note: one part sodium ...
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